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Lammerink, and B. :J . R. Neth. Chem. , 1983, 102,400. g. 9% (E)-geometry. g. ZnXz] ( 3 1 ) X=CL or1 Ph Reagents: i, Zn; ii, [Cp,TiCl,]; iii, Ph Scheme 23 able starting materials, its use is limited by its high reactivity towards other functional groups such as carboxylic acid chlorides, nitriles, benzyl halides, and even acetylenic bonds. 68The most accessible of these, which probably exists as the equilibrium mixture (32), is formed by treating molybdenum pentachloride with two equivalents of methyl-lithium.
E. -T. Luo, J . Org. , 1983,48, 1560. Saturated and Unsaturated Hydrocarbons 31 a,@-Unsaturated aldehydes and ketones can be prepared by direct dehydrogenation of the corresponding saturated carbonyl compounds using silver or tin(I1) triflates, amines, and stoicheiometric amounts of palladium(I1) complexes. 119 Ketones, carboxylic esters, and aliphatic chlorine atoms are inert under the conditions used for the dehydrogenation of aldehydes. 12* 2-Mercaptobenzothiazole is a by-product of the reaction and can be re-cycled.
J. Whittle, J . Chem. , Chem. , 1983, 503. 156 G . Stork and R. , J . A m . Chem. , 1983, 105, 3720. l~~ koH . iv, R (99) Reagents: i, 2Bu"Li; ii, ICH,CO,Na; iii, TsOH; iv, Et,N Scheme 73 Butenolides substituted at the 4-position can be prepared from the appropriate P-hydroxysulphones in the same way. In another approach, dimethoxydihydrofurans (100) , prepared from the corresponding 2-substituted furans (using, for example, bromine and a weak base in methanol), are converted into 157 K. Tanaka, K.