Download Small-Angle Scattering from Confined and Interfacial Fluids: by Yuri B. Melnichenko PDF
By Yuri B. Melnichenko
This booklet examines the meso- and nanoscopic elements of fluid adsorption in porous solids utilizing a non-invasive approach to small perspective neutron scattering (SANS) and small perspective x-ray scattering (SAXS). beginning with a short precis of the elemental assumptions and result of the speculation of small-angle scattering from porous media, the writer specializes in the sensible features and technique of the ambient and excessive strain SANS and SAXS experiments and corresponding information research. it really is illustrated with result of experiences of the vapor and supercritical fluid adsorption in porous fabrics released over the last decade, acquired either for man-made fabrics (e.g. porous fractal silica, Vycor glass, activated carbon) and geological samples (e.g. sandstones, shales and coal). in an effort to serve the wishes of vast readership, the consequences are awarded within the appropriate context (e.g. petroleum exploration, anthropogenic carbon catch and sequestration, ion adsorption in supercapacitors, hydrogen garage, etc.).
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Additional resources for Small-Angle Scattering from Confined and Interfacial Fluids: Applications to Energy Storage and Environmental Science
Sample text
Use of such high-flux beams in SAS research requires significant beam attenuation to avoid sample damage. Even after attenuation and focusing of the 16 1 Basic Definitions and Essential Concepts of Small-Angle Scattering beam down to a few tens of micrometers, the resulting flux on the sample is high enough to ensure counting time on the order of seconds, which allows one to conduct position-sensitive scans and investigate fast kinetic phenomena such as penetration of supercritical CO2 into coal.
SpICE is built on LabVIEW (National Instruments Corporation, Austin, Texas, USA) and provides a simple 42 3 Constant Flux and Time-of-Flight Instrumentation Fig. 6 Image of the 3He detector (front view) command-driven interface for performing all necessary functions of the instrument. org). The user interacts through a graphical user interface (GUI) developed specifically for SANS instruments at HFIR, which provides an easy-to-use interface with integrated real-time feedback. The raw data are saved in XML files containing pertinent instrument-configuration information, and a template style sheet is available for viewing this information in tabular format using a web browser.
Rev. Miner. Geochem. 63, 27 (2006) 4. : Comprehensive upgrade of the high-resolution small-angle neutron scattering instrument KWS-3 at FRM II. J. Appl. Crystallogr. 44, 337 (2011) 5. : Neutron applications in earth, energy and environmental sciences. , Rinaldi, H. ) Neutron Scattering Instrumentation. Springer, New York, NY (2010) 6. : Spallation neutron source moderator design. Phys. Res. A 411, 494 (1998) 7. : Imaging and applications. A reference for the imaging community. Z. ) Neutron Sources and Facilities.